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It could be UAC in Vista. I have it disabled here.
Disabling it for long periods of time is not recommended, but you could try disabling it for times you need to access your PPC\Windows folder.
Edit: I just turned UAC on and tried and I can still see the windows folder and all hidden/rom files in it. The only other thing I can think of is that I was running with UAC off when I created the sync partnership. Or do any of you who are having problems have the extended rom unlocked on your phones? I do here.
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